HCl 600 ml and water 160 ml, organic residue 250 gm of 1 1 Z of 1 N hydroxy 5 methoxy 1 4 trifluoromethyl phenyl pentan 1 imine and traces of 5 methoxy 1 4 trifluoromethyl phenyl pentan 1 one obtained after hexane recovery from stage 1 filtrate was added at temperature 25 30 C under stirring
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